阳离子交换树脂与大孔吸附树脂联用富集桑叶中总生物碱与总酚的工艺研究

留言板

尊敬的读者、作者、审稿人, 关于本刊的投稿、审稿、编辑和出版的任何问题, 您可以本页添加留言。我们将尽快给您答复。谢谢您的支持!

姓名

邮箱

手机号码

标题

留言内容

验证码

Study on Enriching Total Alkaloids and Total Phenols from Mulberry by Cation Exchange Resin and Macroporous Absorption Resin

1.
Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources Industrialization, Nanjing University of Chinese Medicine, Nanjing, 210023, China
2.
Jiangsu Key Laboratory of Research and Development in Marine Bio-resource Pharmaceutics, Nanjing University of Chinese Medicine, Nanjing, 210023, China

摘要: 目的富集桑叶中总生物碱和总酚。方法联合应用阳离子交换树脂和大孔吸附树脂对桑叶中总生物碱和总酚成分进行富集纯化，并对工艺进行优化和验证。结果该工艺可较好的富集纯化桑叶中总生物碱和总酚成分，指标性成分1-脱氧野尻霉素（DNJ）、绿原酸、芦丁的含量可达到0.17%、3.05%、0.92%。结论阳离子交换树脂与大孔吸附树脂联用富集桑叶中总生物碱与总酚的方法可行，适合于大生产。
- 桑叶 /
- 阳离子交换树脂 /
- 大孔吸附树脂 /
- 总生物碱 /
- 总酚
Abstract: OBJECTIVE To enrich the total alkaloids and total phenols from mulberry. METHODS Combined appling cation exchange resin and macroporous absorption resin to enrich and purify the total alkaloids and total phenols， then verify and optimize the process. RESULTS The process contributed to enrich and purify the total alkaloids and total phenols from mulberry. The content of DNJ， chlorogenic acid and rutin can achieve 0.17%， 3.05% and 0.92%. CONCLUSION Using cation exchange resin and macroporous absorption resin to concentration of the total alkaloids and total phenols may be applied for the real bulk production.
- mulberry /
- cation exchange resin /
- macroporous absorption resin /
- total alkaloids /
- total phenols

[1]	丁盈，蒋梅香，周应军，等．桑叶降糖活性成分研究[J]．中国药物化学杂志，2007， 17（6）：386-389．
[2]	Ding Y，Jiang MX， Zhou YJ， et al. Active constituents of lowering blood sugars from Morus alba L[J]. Chin J Med Chem， 2007， 17(6): 386-389.
[3]	常钰. 桑叶降血糖胶囊的研制[D]. 镇江：江苏大学，2008.
[4]	Chang Y. Study on Mullberry Leave Hypoglycemic Capsule[D]. Zhenjiang： Jiangsu University，2008.
[5]	李继文，郭晓燕，王腾，等．荧光衍生化法测定不同季节桑叶中1-脱氧野尻霉素的含量[J]．食品工业科技，2011（12）：462-464， 467．
[6]	Li JW，Guo XY， Wang T， et al. Determination of 1-deoxynojirimycin in Morus alba L.leaves of different seasons by fluorometric derivatization[J]. Sci Technol Food Indust， 2011(12): 462-464， 467.

点击查看大图