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HPLC法同时测定半枝莲中黄酮和生物碱类成分

康安 乔广军 张正伟 郭锦瑞 狄留庆 吴勉华 周红光

康安, 乔广军, 张正伟, 郭锦瑞, 狄留庆, 吴勉华, 周红光. HPLC法同时测定半枝莲中黄酮和生物碱类成分[J]. 南京中医药大学学报, 2013, 29(5): 479-481.
引用本文: 康安, 乔广军, 张正伟, 郭锦瑞, 狄留庆, 吴勉华, 周红光. HPLC法同时测定半枝莲中黄酮和生物碱类成分[J]. 南京中医药大学学报, 2013, 29(5): 479-481.
KANGAn, QIAOGuang-jun, GUOJin-rui, ZHANGZheng-wei, DILiu-qing, WUMian-hua, ZHOUHong-guang. Simultaneous Determination of Flavones and Scutebarbatines in Scutellariae barbatae by HPLC[J]. Journal of Nanjing University of traditional Chinese Medicine, 2013, 29(5): 479-481.
Citation: KANGAn, QIAOGuang-jun, GUOJin-rui, ZHANGZheng-wei, DILiu-qing, WUMian-hua, ZHOUHong-guang. Simultaneous Determination of Flavones and Scutebarbatines in Scutellariae barbatae by HPLC[J]. Journal of Nanjing University of traditional Chinese Medicine, 2013, 29(5): 479-481.

HPLC法同时测定半枝莲中黄酮和生物碱类成分

Simultaneous Determination of Flavones and Scutebarbatines in Scutellariae barbatae by HPLC

  • 摘要: 目的 建立同时测定半枝莲饮片中木犀草素、芹菜素、汉黄芩素、半枝莲生物碱A和半枝莲生物碱B的HPLC法。方法 采用高效液相色谱法,色谱柱为Phenomenon C18柱(250 mm×4.60 mm,5 μm),以乙腈-水溶液为流动相,梯度洗脱;流速为1.0 mL/min,柱温为30 ℃;木犀草素、芹菜素检测波长为355 nm,汉黄芩素、半枝莲生物碱A和生物碱B检测波长为264 nm。结果 木犀草素、芹菜素、汉黄芩素、半枝莲生物碱A和生物碱B分别在0.0374~2.40 μg、0.0312~2.00 μg、0.0312~2.00 μg、0.0062~0.40 μg和0.0062~0.40 μg内线性关系良好。精密度,重复性及加样回收均符合要求。结论 此方法快速简便,重现性好,可用于半枝莲饮片的质量控制。

     

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    [5] Marconett CN, Morgenstern TJ, San Roman AK, et al. BZL101, a phytochemical extract from the Scutellaria barbata plant, disrupts proliferation of human breast and prostate cancer cells through distinct mechanisms dependent on the cancer cell phenotype[J]. Cancer Biol Ther, 2010 , 10(4):397-405.
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出版历程
  • 收稿日期:  2013-07-03
  • 修回日期:  2013-08-21
  • 刊出日期:  2013-09-10

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